JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 31

Material selection For the study, Ticona supplied 0.25-mm thick PP/glass UD tapes (Celstran CFRTP PP-GF70 with 70 wt-% glass) in a variety of widths. Although such tapes are available in a variety of thicknesses, in practice, they are not stiff enough to handle easily, particularly in an automated or semi-automated moulding process, making it more likely the tapes will move during moulding and end up in locations other than those needing property improvements. Hence, such tapes are generally converted into an intermediate form like a fabric or a tailored laminate before use. Oxeon converted them into tape fabrics (TeXtreme plain weaves that were 0.50mm thick per ply and were laid up two plies thick in either a 0°/90° = (0/90) or a ± 45° = (± 45) configuration). These double plies were used to build stacked configurations in specific thicknesses that were not preconsolidated. Fiberforge also used the tapes to produce tailored laminates (consolidated tailored blanks). For Part 1 (the plaque study), the laminates were supplied in single sheets (to be cut as needed) and several thicknesses and configurations, e.g. 0°/90° = (0/90) with a thickness of 0.5, 1.0 or 2.0 mm, or a quasi-isotropic (0°/90°/+45°/-45°)s where “s” represents a symmetric layup of eight plies. For Part 2 (the engine-shield study), both partshape tailored laminates and large sheets of laminate were produced, which were then cut to size and shape as needed. In both cases, the tape laminates were preconsolidated. Preheating and moulding conditions The tape fabrics and tailored laminates were used alone or paired with a D-LFT composite produced by Fraunhofer, with an ILC unit supplied by Dieffenbacher GmbH Maschinen- und Anlagenbau, PP resin from Dow Chemical, an additives package from Addcomp Holland BV, and chopped-glass fibre by Johns Manville. For the plaque study, glass loading was 30 wt-% (a common automotive formulation), but for the shield study, 20 wt-% was used to enhance fill of more complex geometry.

Both plaque and shield tools were moulded on a Dieffenbacher 36,000kN Compress Plus hydraulic press with parallel levelling control. In all cases where hybrid combinations of D-LFT charge, tape fabric and/or tailored laminate were used, the D-LFT charge was always placed in the tool last and laid on top of tape fabric and/or tape laminate. To ensure good fusion between the D-LFT charge (which exits the ILC unit near 200°C) and the tape fabric and/or tailored laminates, the latter were preheated in an infrared oven close to 200°C. For unconsolidated fabrics, individual plies were pre-stacked (without additional pressure) in the oven prior to heating. Since a range of thicknesses were investigated in the plaque study, preheating times ranged from 30-140 seconds, while materials for the shield tool took 60 seconds. Heating times were governed by the oven, whose power was set so as not to degrade the surface of UD-tape products before resin at the core reached processing temperatures. Use of optimized heating setups could lower preheat times significantly.

Phase 1: plaque moulding trials and impact testing For Phase 1, a total of 20 material/layup combinations were successfully produced, the most representative of which are shown in Table 1 (pure D-LFT, pure tape laminate, pure tape fabric and several hybrid configurations). Plaques were moulded at ≈3,200 kN pressure for 45 seconds at 75°C. Since many plaques were 3.0-mm thick, a longer dwell time was needed to chill parts sufficiently for demoulding. Although thinner layups could have been moulded faster, researchers felt it best to keep process conditions the same, so left all plaques in the tool 45 seconds. At least one plaque was produced for each combination (for hybrid layups, two plaques were produced). After moulding, test coupons were cut from plaques and subjected to instrumented puncture impact testing as per EN ISO 6603-2 “Determination of multiaxial impact behaviour of rigid plastics – Part 2: Instrumented puncture test.” For each configuration, at least 5 samples were impacted

Tab. 1: Selected materials/layup/orientation/thicknesses used to mould flat test plaques in the first section of the study (n/a = not applicable for this sample)

Hybrid layup combinations

Materials used
Pure tape fabric Pure tape laminate Pure D-LFT Pure D-LFT Pure D-LFT Hybrid of tape fabric + D-LFT Hybrid of tape laminate + D-LFT Hybrid of tape fabric + D-LFT Hybrid of tape laminate+ D-LFT Hybrid of tape fabric + tape laminate + D-LFT Hybrid of tape laminate + tape fabric + D-LFT

Nominal wall (mm)
2.0 2.0 2.0 2.5 3.0 0.5 + 2.5 0.5 + 2.5 1.0 + 2.0 1.0 + 2.0

No. of plies/ layers 4 1
n/a n/a n/a 1 1 2 1

Fibre orientation of each ply (o) (0/90) (0/90)2s
D-LFT D-LFT

V1 V2
V3 V4 V5 V6 V7 V8 V9 V10

Feature Automotive

D-LFT (0/90) + D-LFT (0/90) + D-LFT 2x(0/90) + D-LFT (0/90)s + D-LFT (0/90) + (0/90) + D-LFT (0/90) + (0/90) + D-LFT

2 x 0.5 + 2.0

1+1

V11

2 x 0.5 + 2.0

1+1

No74 July 2012 /

jec composites magazine 31



JEC COMPOSITES MAGAZINE - Issue #74 - July 2012

Table of Contents for the Digital Edition of JEC COMPOSITES MAGAZINE - Issue #74 - July 2012

Cover
Edito
Point of view: Closer to the shop floor
Contents
Agenda of Events
COMPANY & BUSINESS
- In Brief
- Glass fibre
APPLICATIONS
- Pipes & tanks
- Building
MARKET
- Human resources
- Glass fibre
- Turkey
FEATURE AUTOMOTIVE
- Braiding
- Lightening
- D-LFT
- Sustainability
- RTM
- RIM
RESEARCH & DEVELOPMENT
- Design
- Fatigue behaviour
TECHNOLOGY & INNOVATIONS
- Wind
- Reinforcement
Index
In the world
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - Cover
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 2
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - Edito
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - Point of view: Closer to the shop floor
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 5
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - Contents
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 7
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - Agenda of Events
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - In Brief
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Glass fibre
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 11
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 12
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Pipes & tanks
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Building
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 15
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 16
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 17
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Human resources
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Glass fibre
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 20
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 21
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Turkey
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 23
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Braiding
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 25
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Lightening
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 27
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 28
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 29
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - D-LFT
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 31
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 32
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 33
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Sustainability
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 35
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 36
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - RTM
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 38
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 39
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - RIM
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Design
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 42
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 43
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 44
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 45
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Fatigue behaviour
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 47
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 48
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 49
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 50
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Wind
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 52
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 53
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - - Reinforcement
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 55
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 56
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - Index
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - In the world
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 59
JEC COMPOSITES MAGAZINE - Issue #74 - July 2012 - 60
https://www.nxtbook.fr/newpress/jeccomposites/jcm2107_141
https://www.nxtbook.fr/newpress/jeccomposites/jcm2105_140
https://www.nxtbook.fr/newpress/jeccomposites/jcm2103_139
https://www.nxtbook.fr/newpress/jeccomposites/jcm-experts-digest-additive-manufacturing-2020
https://www.nxtbook.fr/newpress/jeccomposites/jcm2101_138
https://www.nxtbook.fr/newpress/jeccomposites/jcm2011_Special_Issue4
https://www.nxtbook.fr/newpress/jeccomposites/jcm2011_137
https://www.nxtbook.fr/newpress/jeccomposites/jcm2009_136
https://www.nxtbook.fr/newpress/jeccomposites/jcm2007_135
https://www.nxtbook.fr/newpress/jeccomposites/jcm_2020_Q1_Innovation_Report
https://www.nxtbook.fr/newpress/jeccomposites/jcm2005_Special_Issue3
https://www.nxtbook.fr/newpress/jeccomposites/jcm2005_134
https://www.nxtbook.fr/newpress/jeccomposites/jcm2003_133
https://www.nxtbook.fr/newpress/jeccomposites/jcm2001_132
https://www.nxtbook.fr/newpress/jeccomposites/jcm1911_Special_Issue2
https://www.nxtbook.fr/newpress/jeccomposites/jcm1911_131
https://www.nxtbook.fr/newpress/jeccomposites/jcm1909_130
https://www.nxtbook.fr/newpress/jeccomposites/jcm1907_129
https://www.nxtbook.fr/newpress/jeccomposites/jcm1905_128
https://www.nxtbook.fr/newpress/jeccomposites/jcm1903_Special_Issue1
https://www.nxtbook.fr/newpress/jeccomposites/jcm1903_127
https://www.nxtbook.fr/newpress/jeccomposites/jcm1901_126
https://www.nxtbook.fr/newpress/jeccomposites/jcm1811_125
https://www.nxtbook.fr/newpress/jeccomposites/jcm1810_124
https://www.nxtbook.fr/newpress/jeccomposites/jcm1808_123
https://www.nxtbook.fr/newpress/jeccomposites/jcm1807_122
https://www.nxtbook.fr/newpress/jeccomposites/jcm1805_121
https://www.nxtbook.fr/newpress/jeccomposites/jcm1804_120
https://www.nxtbook.fr/newpress/jeccomposites/jcm1803_119
https://www.nxtbook.fr/newpress/jeccomposites/jcm1802_119-Supplement_Innovation_Report
https://www.nxtbook.fr/newpress/jeccomposites/jcm1801_118
https://www.nxtbook.fr/newpress/jeccomposites/jcm1711_117
https://www.nxtbook.fr/newpress/jeccomposites/jcm1710_116
https://www.nxtbook.fr/newpress/jeccomposites/jcm1708_115
https://www.nxtbook.fr/newpress/jeccomposites/jcm1707_114
https://www.nxtbook.fr/newpress/jeccomposites/jcm1706_113
https://www.nxtbook.fr/newpress/jeccomposites/jcm1704_112
https://www.nxtbook.fr/newpress/jeccomposites/jcm1703_111
https://www.nxtbook.fr/newpress/jeccomposites/jcm1701_110
https://www.nxtbook.fr/newpress/jeccomposites/jcm1611_109
https://www.nxtbook.fr/newpress/jeccomposites/jcm1610_108
https://www.nxtbook.fr/newpress/jeccomposites/jcm1608_107
https://www.nxtbook.fr/newpress/jeccomposites/jcm1607_106
https://www.nxtbook.fr/newpress/jeccomposites/jcm1605_105
https://www.nxtbook.fr/newpress/jeccomposites/jcm1604_104
https://www.nxtbook.fr/newpress/jeccomposites/jcm1603_103
https://www.nxtbook.fr/newpress/jeccomposites/jcm1601_102
https://www.nxtbook.fr/newpress/jeccomposites/jcm1511_101
https://www.nxtbook.fr/newpress/jeccomposites/jcm1510_100
https://www.nxtbook.fr/newpress/jeccomposites/jcm1509_99
https://www.nxtbook.fr/newpress/jeccomposites/jcm1507_98
https://www.nxtbook.fr/newpress/jeccomposites/jcm1505_97
https://www.nxtbook.fr/newpress/jeccomposites/jcm1504_96
https://www.nxtbook.com/newpress/jeccomposites/jcm1503_95
https://www.nxtbook.com/newpress/jeccomposites/jcm1501_94
https://www.nxtbook.com/newpress/jeccomposites/jcm1412_93
https://www.nxtbook.com/newpress/jeccomposites/jcm1410_92
https://www.nxtbook.com/newpress/jeccomposites/jcm1409_91
https://www.nxtbook.com/newpress/jeccomposites/jcm1406_90
https://www.nxtbook.com/newpress/jeccomposites/jcm1405_89
https://www.nxtbook.com/newpress/jeccomposites/jcm1404_88
https://www.nxtbook.com/newpress/jeccomposites/jcm1403_87
https://www.nxtbook.com/newpress/jeccomposites/jcm1401_86
https://www.nxtbook.com/newpress/jeccomposites/jcm1311_85
https://www.nxtbook.com/newpress/jeccomposites/jcm1310_84
https://www.nxtbook.com/newpress/jeccomposites/jcm1308_83
https://www.nxtbook.com/newpress/jeccomposites/jcm1307_82
https://www.nxtbook.com/newpress/jeccomposites/jcm1305_81
https://www.nxtbook.com/newpress/jeccomposites/jcm1304_80
https://www.nxtbook.com/newpress/jeccomposites/jcm1303_79
https://www.nxtbook.com/newpress/jeccomposites/jcm1301_78
https://www.nxtbook.com/newpress/jeccomposites/jcm1212_77
https://www.nxtbook.com/newpress/jeccomposites/jcm1210_76
https://www.nxtbook.com/newpress/jeccomposites/jcm1208_75
https://www.nxtbook.com/newpress/jeccomposites/jcm1207_74
https://www.nxtbook.com/newpress/jeccomposites/jcm1206_73
https://www.nxtbook.com/newpress/jeccomposites/jcm1204_72
https://www.nxtbook.com/newpress/jeccomposites/jcm1203_71
https://www.nxtbook.com/newpress/jeccomposites/jcm1201_70
https://www.nxtbook.com/newpress/jeccomposites/jcm1111_69
https://www.nxtbook.com/newpress/jeccomposites/jcm1110_68
https://www.nxtbook.com/newpress/jeccomposites/jcm1108_67
https://www.nxtbook.com/newpress/jeccomposites/jcm1107_66
https://www.nxtbook.com/newpress/jeccomposites/jcm1105_65
https://www.nxtbook.com/newpress/jeccomposites/jcm1104_64
https://www.nxtbook.com/newpress/jeccomposites/jcm1103_63
https://www.nxtbook.com/newpress/jeccomposites/jcm1101_62
https://www.nxtbook.com/newpress/jeccomposites/jcm1011_61
https://www.nxtbook.com/newpress/jeccomposites/jcm1010_60
https://www.nxtbook.com/newpress/jeccomposites/jcm1009_59
https://www.nxtbook.com/newpress/jeccomposites/jcm1006_58
https://www.nxtbook.com/newpress/jeccomposites/jcm1005_57
https://www.nxtbook.com/newpress/jeccomposites/jcm1004_56
https://www.nxtbook.com/newpress/jeccomposites/jcm1003_55
https://www.nxtbook.com/newpress/jeccomposites/jcm1001_54
https://www.nxtbook.com/newpress/jeccomposites/jcm0911_53
https://www.nxtbook.com/newpress/jeccomposites/jcm0910_52
https://www.nxtbook.com/newpress/jeccomposites/jcm0909_51
https://www.nxtbook.com/newpress/jeccomposites/jcm0907-08_50
https://www.nxtbook.com/newpress/jeccomposites/jcm0906_49
https://www.nxtbook.com/newpress/jeccomposites/jcm0904_48
https://www.nxtbook.com/newpress/jeccomposites/jcm0903_47
https://www.nxtbook.com/newpress/jeccomposites/jcm0901_46
https://www.nxtbook.com/newpress/jeccomposites/jcm0811_45
https://www.nxtbook.com/newpress/jeccomposites/jcm0810_44
https://www.nxtbook.com/newpress/jeccomposites/jcm0809_43
https://www.nxtbook.com/newpress/jeccomposites/jcm0807_42
https://www.nxtbook.com/newpress/jeccomposites/jcm0806_41
https://www.nxtbook.com/newpress/jeccomposites/jcm0805_40
https://www.nxtbook.com/newpress/jeccomposites/jcm0803_39
https://www.nxtbook.com/newpress/jeccomposites/jcm0801_38
https://www.nxtbook.com/newpress/jeccomposites/jcm0712_37
https://www.nxtbook.com/newpress/jeccomposites/jcm0710_36
https://www.nxtbook.com/newpress/jeccomposites/jcm0709_35
https://www.nxtbook.com/newpress/jeccomposites/jcm0707_34
https://www.nxtbook.com/newpress/jeccomposites/jcm0706_33
https://www.nxtbookmedia.com